Oxidation and SCC initiation studies of type 304L SS in PWR primary water

F. Scenini, J. Lindsay, Litao Chang, Y. L. Wang, M. G. Burke, S. Lozano-Perez, G. Pimentel, D. Tice, K. Mottershead, V. Addepalli

Research output: Chapter in Book/Report/Conference proceedingConference contributionpeer-review

3 Scopus citations

Abstract

Slow strain rate tensile (SSRT) tests were conducted on conventional and tapered samples manufactured from forged Type 304L stainless steel to assess the stress corrosion cracking (SCC) behaviour in simulated PWR primary water. Several testing and microstructural parameters were investigated in order to explore the conditions under which crack initiation might occur. Surface preparation appeared to play a very important role on SCC initiation whereby the machined surfaces were the least susceptible to SCC initiation whilst oxide polishing suspension (OPS) polished surfaces were more susceptible. On the machined surfaces the cracks were always transgranular (TG) in nature and associated with the machining marks. Conversely, on fine polished surfaces with oxide polishing suspension the crack morphology was mainly intergranular in nature, although minor transgranular cracking was observed. The regions in the proximity of the δ-ferrite/austenite interface were shown to be very susceptible to SCC initiation especially on the OPS polished surfaces and this was attributed to the strain localization upon dynamic deformation. Furthermore, intragranular inclusions appeared to dissolve and act as initiation sites for transgranular cracking to occur. The roles of strain rate, dynamic deformation and microstructure on the initiation of SCC are also discussed.

Original languageEnglish
Title of host publicationMinerals, Metals and Materials Series
PublisherSpringer International Publishing
Pages793-810
Number of pages18
ISBN (Print)9783030046385, 9783030046392, 9783319515403, 9783319651354, 9783319728520, 9783319950211
DOIs
StatePublished - 2019
Externally publishedYes
Event18th International Conference on Environmental Degradation of Materials in Nuclear Power Systems – Water Reactors 2019 - Boston, United States
Duration: Aug 18 2019Aug 22 2019

Publication series

NameMinerals, Metals and Materials Series
ISSN (Print)2367-1181
ISSN (Electronic)2367-1696

Conference

Conference18th International Conference on Environmental Degradation of Materials in Nuclear Power Systems – Water Reactors 2019
Country/TerritoryUnited States
CityBoston
Period08/18/1908/22/19

Keywords

  • 304L stainless steel
  • Oxidation
  • Slow strain rate test (SSRT)
  • Stress corrosion cracking (SCC) initiation

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